化工社化工社 化学情報印刷レポート · 研究参考用
6-Bromohexanoyl chloride → 9-(6-Bromohexanoyl)-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Bromohexanoyl chloride | HCID 89848 | — |
| 反応物 | 1,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one | HCID 13694564 | — |
| 生成物 | 9-(6-Bromohexanoyl)-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one | HCID 21887435 | — |
反応手順
Using 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one and 6-bromohexanoyl chloride according to the same method as that of Reference Example 1, the title compound (3.90 g) was obtained as colorless crystals having a melting point of 52–53° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07132547B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-2f29cb0b09d64b149635a812a8726aa1 |
| 出典メモ | uspto-grants-2006_11 |