化工社化工社 化学情報印刷レポート · 研究参考用
1-Bromo-4-nitrobenzene → 4-Nitro-1,1'-biphenyl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Bromo-4-nitrobenzene | HCID 11466 | — |
| 反応物 | Phenylboronic Acid | HCID 66827 | — |
| 生成物 | 4-Nitro-1,1'-biphenyl | HCID 7114 | — |
反応手順
4-Nitro-bromobenzene and phenyl boronic acid were reacted as described in Example 6. The catalyst was recovered by filtration, washed and dried (as described in Example 1). This process was then repeated 4 times with fresh reagents and the recycled catalyst. The yields of isolated 4-Nitrobiphenyl were as follows:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08828902B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-05b04c0b57cb4631982c99303f558e8c |
| 出典メモ | uspto-grants-2014_09 |