関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | L-Phenylalanine | HCID 6140 | — |
| 反応物 | Butyric anhydride | HCID 7798 | — |
| 生成物 | Phenylalanine butyramide | HCID 68631493 | — |
反応手順
5 g of phenylalanine was added to 20 mL of butyric anhydride and the resulting mixture heated to about 100° C. for about 3 h. Excess butyric anhydride was then removed under reduced pressure to provide a solid residue that was recrystallized from ethanol to provide phenylalanine butyramide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08828960B2 |
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| 出典データセット | uspto-grants-2014_09 |
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| ORD ID | ord-3e84eb0ed57b475cbbdee34bf3c5aaeb |
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| 出典メモ | uspto-grants-2014_09 |
|---|