化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 1-Benzyl-3-methylpyrrolidin-3-amine dihydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | N-(1-benzyl-3-methylpyrrolidin-3-yl)acetamide | HCID 13787481 | — |
| 生成物 | 1-Benzyl-3-methylpyrrolidin-3-amine dihydrochloride | HCID 66884810 | — |
反応手順
A mixture of N-(1-benzyl-3-methylpyrrolidin-3-yl)acetamide (4.01 g, 17.2 mmol) and conc HCl (50 mL) was heated at reflux for 2 d. The mixture was evaporated under reduced pressure to leave 1-benzyl-3-methylpyrrolidin-3-amine dihydrochloride salt as a brown tar.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08828985B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-310dbf237d6e40efa44cc49107bad530 |
| 出典メモ | uspto-grants-2014_09 |