化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyl Carbonate → Methyl triflate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Carbonate | HCID 12021 | — |
| 反応物 | Trifluoromethanesulfonic anhydride | HCID 67749 | — |
| 生成物 | Methyl triflate | HCID 9526 | 197.7% |
反応手順
731 g (2.59 mol) of trifluoromethanesulfonic anhydride and 232 g (2.58 mol) of dimethyl carbonate are added to the residue, and the process described above is repeated. 837 g of methyl trifluoromethanesulfonate having a purity of greater than 99% are isolated (yield: 99.1%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07084290B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-befbfb3aff7c451d95620ddeb9864f61 |
| 出典メモ | uspto-grants-2006_08 |