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HRID 722202作成日:2026年10月26日

2-Chloro-4,5-difluorobenzoyl Isocyanate → HCID 178488186、化合物

https://huagongshe.com/reaction/722202

反応式

関与物質

役割名称HCID仕込み量
反応物2-Chloro-4,5-difluorobenzoyl IsocyanateHCID 11557583—
反応物HCID 178488184HCID 178488184—
溶媒AcetonitrileHCID 6342—
生成物HCID 178488186HCID 178488186—

反応手順

The solution of equivalent amounts of 2-chloro-4,5-difluorobenzoyl isocyanate was added dropwise to the solution of 30 mg of 2-methoxy-4-(5-methyl-4H-[1,2,4]triazol-3-yl)phenylamine in 3 ml of acetonitrile and the mixture was stirred at room temperature for 30 minutes. The solid was then filtered off with suction, stirred with isopropanol and dried under reduced pressure.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07138414B2
出典データセットuspto-grants-2006_11
ORD IDord-9d63ce9c4ae741549cc6f9bc5d723dc6
出典メモuspto-grants-2006_11