Dihydro-2-methyl-3(2H)-furanone → HCID 86628968、化合物

HRID 72226

反応式

HRID 72226 の反応式
[CH3:1][O:2][C:3]([C:5]1[S:6][CH:7]=[CH:8][C:9]=1[NH:10][C:11](=[O:16])[C:12]([F:15])([F:14])[F:13])=[O:4].[CH3:17][CH:18]1[C:22](=[O:23])[CH2:21][CH2:20][O:19]1>>[CH3:1][O:2][C:3]([C:5]1[S:6][C:7]([C:22]2([OH:23])[CH2:21][CH2:20][O:19][CH:18]2[CH3:17])=[CH:8][C:9]=1[NH:10][C:11](=[O:16])[C:12]([F:13])([F:14])[F:15])=[O:4]

参加物

3

反応物 2

HCID 18522Dihydro-2-methyl-3(2H)-furanoneHCID 2805185Methyl 3-(2,2,2-trifluoroacetamido)thiophene-2-carboxylate

生成物 1

HCID 86628968HCID 86628968、化合物

実験手順

3-(2,2,2-Trifluoroacetylamino)thiophene-2-carboxylic acid methyl ester and 2-methyldihydrofuran-3-one were reacted by method M. The product with the molecular weight of 353.32 (C13H14F3NO5S) was obtained in this way; MS (ESI): 354 (M+H+).

後処理

  1. customThe product with the molecular weight of 353.32 (C13H14F3NO5S) was obtained in this way

出典と根拠

ORDレコード
ord-bdd358f983d44b5bb111eda67d0b1952
出典データセット
uspto-grants-2014_09
特許番号
US08828991B2

関連ノート

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