化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-4-(trifluoromethyl)phenol → N-(2-Hydroxy-5-trifluoromethylphenyl)-2-fluoro-5-nitrobenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-(trifluoromethyl)phenol | HCID 120246 | — |
| 反応物 | 2-Fluoro-5-nitrobenzoyl chloride | HCID 10976570 | — |
| 生成物 | N-(2-Hydroxy-5-trifluoromethylphenyl)-2-fluoro-5-nitrobenzamide | HCID 21884558 | — |
反応手順
Prepared by the method of Example 15a), from 2-amino-4-trifluoromethylphenol (407 mg, 2.3 mmol) and 2-fluoro-5-nitrobenzoyl chloride (468 mg, 2.3 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07138425B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-d529938645dc4604aa966d30da2ea4c8 |
| 出典メモ | uspto-grants-2006_11 |