Propylamine → 2-(3-Nitro-6-propylaminophenyl)-5-trifluoromethylbenzoxazole

HRID 722582

反応式

HRID 722582 の反応式
[N+:1]([C:4]1[CH:5]=[C:6]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:14]=3[N:15]=2)[C:7](F)=[CH:8][CH:9]=1)([O-:3])=[O:2].[CH2:24]([NH2:27])[CH2:25][CH3:26]>>[N+:1]([C:4]1[CH:5]=[C:6]([C:11]2[O:12][C:13]3[CH:19]=[CH:18][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:16][C:14]=3[N:15]=2)[C:7]([NH:27][CH2:24][CH2:25][CH3:26])=[CH:8][CH:9]=1)([O-:3])=[O:2]

参加物

3

反応物 2

HCID 7852PropylamineHCID 218845112-(3-Nitro-6-fluorophenyl)-5-trifluoromethylbenzoxazole

生成物 1

HCID 218844522-(3-Nitro-6-propylaminophenyl)-5-trifluoromethylbenzoxazole

実験手順

Prepared by the method of Example 54a), from 2-(3-nitro-6-fluorophenyl)-5-trifluoromethylbenzoxazole (218 mg, 0.8 mmol) and propylamine (328 μL, 4.0 mmol) the subtitle compound was obtained. The product was used directly in the next step without purification.

出典と根拠

ORDレコード
ord-716874ddafe94509b9351849d8054af9
出典データセット
uspto-grants-2006_11
特許番号
US07138425B2

関連ノート

読み込み中…