化工社化工社 化学情報印刷レポート · 研究参考用
6-Bromohexanoyl chloride → 8-(6-Bromohexanoyl)-1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Bromohexanoyl chloride | HCID 89848 | — |
| 反応物 | Pyroquilon | HCID 91665 | — |
| 生成物 | 8-(6-Bromohexanoyl)-1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one | HCID 21887546 | — |
反応手順
Using 1,2,5,6-tetrahydro-4H-pyrrolo[3,2,1-ij]quinolin-4-one (3.00 g) and 6-bromohexanoyl chloride (2,91 ml) according to the same method as that of Reference Example 1, the title compound (3.94 g) was obtained as white crystals having a melting point of 97 to 98° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07138533B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-df1ee297ab0c4b76af5881916bb6b0b6 |
| 出典メモ | uspto-grants-2006_11 |