関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | (Chlorothio)formyl chloride | HCID 75990 | — |
| 反応物 | 4-Benzyloxybenzamide | HCID 2726431 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 5-(4-Benzyloxyphenyl)-[1,3,4]oxathiazol-2-one | HCID 59549525 | — |
反応手順
4-benzyloxybenzamide (0.66 g, 2.98 mmol) and 0.26 ml of chlorocarbonyl sulfenyl chloride were dissolved in 10 ml of benzene, refluxed for 3 hours, and stirred at 50° C. for 12 hours. The organic solvent was distilled off under reduced pressure, and the resulting solid was washed with n-hexane to obtain 0.78 g of 5-(4-benzyloxy-phenyl)-[1,3,4]oxathiazol-2-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08828992B2 |
|---|
| 出典データセット | uspto-grants-2014_09 |
|---|
| ORD ID | ord-fbc85fb8b0574939b8b9d725112b0166 |
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| 出典メモ | uspto-grants-2014_09 |
|---|
