Benzaldehyde → HCID 67136987、化合物
反応式
[O:1]([C:8]1[CH:13]=[CH:12][C:11]([NH:14][NH2:15])=[CH:10][CH:9]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:16](=O)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>CO>[CH:16](=[N:15][NH:14][C:11]1[CH:12]=[CH:13][C:8]([O:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[CH:9][CH:10]=1)[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1参加物
4
実験手順
A suspension of (4-phenoxyphenyl)hydrazine (J. Org. Chem. 1956, 395; 1.5 g) in methanol (10 mL) was mixed with benzaldehyde (0.76 mL) and heated to reflux. The crystals which separated out on cooling were filtered off with suction. The product with the molecular weight of 288.35 (C19H16N2O); MS (ESI): 289 ([M+H]+), was obtained in this way.
後処理
- temperatureheated to reflux
- customThe crystals which separated out
- temperatureon cooling
- filtrationwere filtered off with suction
- customMS (ESI): 289 ([M+H]+), was obtained in this way
出典と根拠
- ORDレコード
- ord-559485146324438eaa0a475c3a734b00
- 出典データセット
- uspto-grants-2006_11
- 特許番号
- US07141561B2
反応ノート
読み込み中…