Methylamine → 1-(4-Cyclopentyloxyphenyl)-3-[4-(2-methylaminoethoxy)phenyl]-1,3-dihydroimidazol-2-one

HRID 723368

反応式

HRID 723368 の反応式
Br[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][C:8]([N:11]2[CH:15]=[CH:14][N:13]([C:16]3[CH:21]=[CH:20][C:19]([O:22][CH:23]4[CH2:27][CH2:26][CH2:25][CH2:24]4)=[CH:18][CH:17]=3)[C:12]2=[O:28])=[CH:7][CH:6]=1.[CH3:29][NH2:30]>>[CH:23]1([O:22][C:19]2[CH:20]=[CH:21][C:16]([N:13]3[CH:14]=[CH:15][N:11]([C:8]4[CH:7]=[CH:6][C:5]([O:4][CH2:3][CH2:2][NH:30][CH3:29])=[CH:10][CH:9]=4)[C:12]3=[O:28])=[CH:17][CH:18]=2)[CH2:27][CH2:26][CH2:25][CH2:24]1

参加物

3

反応物 2

HCID 6329MethylamineHCID 218733301-[4-(2-Bromoethoxy)phenyl]-3-(4-cyclopentyloxyphenyl)-1,3-dihydroimidazol-2-one

生成物 1

HCID 218735101-(4-Cyclopentyloxyphenyl)-3-[4-(2-methylaminoethoxy)phenyl]-1,3-dihydroimidazol-2-one

実験手順

1-[4-(2-Bromoethoxy)phenyl]-3-(4-cyclopentyloxyphenyl)-1,3-dihydroimidazol-2-one was reacted with methylamine as described in example 6. The product with the molecular weight of 393.49 (C23H27N3O3); MS (ESI): 394 ([M+H]+) was obtained in this way.

後処理

  1. customMS (ESI): 394 ([M+H]+) was obtained in this way

出典と根拠

ORDレコード
ord-b81ad123f48f4372b6cd4a8aef247eb1
出典データセット
uspto-grants-2006_11
特許番号
US07141561B2

関連ノート

読み込み中…