反応式
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]([C:13]3[CH:18]=[CH:17][C:16]([O:19][C:20]4[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=4)=[CH:15][CH:14]=3)[C:9]2=[O:26])=[CH:4][CH:3]=1.[N:27]1([CH2:33][C:34](O)=[O:35])[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]1>>[O:26]=[C:9]1[N:10]([C:13]2[CH:18]=[CH:17][C:16]([O:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)=[CH:15][CH:14]=2)[CH:11]=[CH:12][N:8]1[C:5]1[CH:4]=[CH:3][C:2]([NH:1][C:34](=[O:35])[CH2:33][N:27]2[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]2)=[CH:7][CH:6]=1参加物
3
実験手順
1-(4-Aminophenyl)-3-(4-phenoxyphenyl)-1,3-dihydroimidazol-2-one was reacted with piperidin-1-ylacetic acid as described in example 217. The product with the molecular weight of 468.56 (C28H28N4O3); MS (ESI): 469 ([M+H]+) was obtained as hydrotrifluoroacetate in this way.
後処理
- customMS (ESI): 469 ([M+H]+) was obtained as hydrotrifluoroacetate in this way
出典と根拠
- ORDレコード
- ord-5a55c84b3b724d5c962033c2618d99df
- 出典データセット
- uspto-grants-2006_11
- 特許番号
- US07141561B2
関連ノート
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