化工社化工社 化学情報印刷レポート · 研究参考用
3-Fluorophenol → (R)-tert-butyl 3-(3-fluorophenoxy)pyrrolidine-1-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Fluorophenol | HCID 9743 | — |
| 反応物 | tert-Butyl (3S)-3-hydroxypyrrolidine-1-carboxylate | HCID 854055 | — |
| 生成物 | (R)-tert-butyl 3-(3-fluorophenoxy)pyrrolidine-1-carboxylate | HCID 67958316 | 98.1% |
反応手順
The title compound (D47) (294.6 mg) was prepared according to the experimental procedure described in Description 40 starting from (S)-tert-butyl 3-hydroxypyrrolidine-1-carboxylate (200 mg, 1.068 mmol, available at Aldrich#634786) and 3-Fluorophenol (0.096 ml, 1.068 mmol).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08828987B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-432db41749aa47bd8c0968977931ddc4 |
| 出典メモ | uspto-grants-2014_09 |