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Aniline → 4-Nitrodiphenylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Aniline | HCID 6115 | — |
| 反応物 | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| 反応物 | Formanilide | HCID 7671 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 溶媒 | Formic Acid | HCID 284 | — |
| 生成物 | 4-Nitrodiphenylamine | HCID 13271 | — |
反応手順
formanilide method, where formic acid and aniline are used as starting materials to prepare formanilide, which in turn reacts with p-nitro-chlorobenzene in the presence of an acid-binding agent such as potassium carbonate, to produce 4-nitrodiphenylamine, and then, 4-nitrodiphenylamine is reduced by sodium sulfide to form 4-aminodiphenylamine;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07084302B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-7a9eeef338d34ed09b7439bf73611b0e |
| 出典メモ | uspto-grants-2006_08 |