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HRID 7265作成日:2026年10月23日

Nitrite → N-Nitrosodiphenylamine

https://huagongshe.com/ja/reaction/7265

反応式

関与物質

役割名称HCID仕込み量
反応物NitriteHCID 946—
反応物DiphenylamineHCID 11487—
生成物N-NitrosodiphenylamineHCID 6838—

反応手順

diphenylamine method, where diphenylamine as raw material is nitrosated using a nitrite in an organic solvent to produce N-nitrosodiphenylamine, which is rearranged to 4-nitrosodiphenylamine hydrochloride under the action of anhydrous hydrogen chloride, and then, 4-nitrosodiphenylamine hydrochloride is neutralized with a base to give 4-nitrosodiphenylamine which is finally reduced to 4-aminodiphenylamine by sodium sulfide.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07084302B2
出典データセットuspto-grants-2006_08
ORD IDord-e70b01ed6e6a4bcc904277bc74d3110e
出典メモuspto-grants-2006_08