3,5,5-Trimethyl-1-hexanol → Hexanoic acid, 3,5,5-trimethyl-, 3,5,5-trimethylhexyl ester

反応式

[CH3:1][CH:2]([CH2:7][C:8]([CH3:11])([CH3:10])[CH3:9])[CH2:3][C:4]([OH:6])=[O:5].[CH3:12][CH:13]([CH2:17][C:18]([CH3:21])([CH3:20])[CH3:19])[CH2:14][CH2:15]O>>[CH3:12][CH:13]([CH2:17][C:18]([CH3:21])([CH3:20])[CH3:19])[CH2:14][CH2:15][O:5][C:4](=[O:6])[CH2:3][CH:2]([CH3:1])[CH2:7][C:8]([CH3:10])([CH3:9])[CH3:11]

参加物

反応物 2

HCID 189383,5,5-Trimethyl-1-hexanol

HCID 909603,5,5-Trimethylhexanoic acid

生成物 1

HCID 100986Hexanoic acid, 3,5,5-trimethyl-, 3,5,5-trimethylhexyl ester

実験手順

The preparation from 3,5,5-trimethylhexanoic acid and 3,5,5-trimethylhexanol was analogous to Example 3; colorless liquid of medium viscosity; B.P. (1.3 mbar=134°-138° C.

後処理

custom1.3 mbar=134°-138° C.

出典と根拠

ORDレコード: ord-38d1dce6670c47c589c5ec131d05cd72
出典データセット: uspto-grants-1998_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05711939

反応ノート

読み込み中…