Hexacyanocobalt → HCID 11125012、化合物

HRID 726941ノート

反応式

HRID 726941 の反応式
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参加物

4

反応物 2

HCID 407334HexacyanocobaltHCID 3007855Zincchloride

生成物 1

HCID 11125012HCID 11125012、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒3 回

実験手順

Potassium hexacyanocobaltate (4.0 g) is dissolved in deionized water (150 mL) in a beaker. Zinc chloride (10 g) is dissolved in deionized water (15 mL) in a second beaker. The aqueous solutions are quickly combined and magnetically stirred for 10 min. The precipitated solids are isolated by centrifugation. The solids are reslurried in deionized water (100 mL) for 10 min. with stirring, and are again recovered by centrifugation. The catalyst is dried in a vacuum oven at 50° C. and 30 in. (Hg) to constant weight. This catalyst is identified as Catalyst A, and has the powder X-ray diffraction pattern shown in FIG. 4.

後処理

  1. customThe precipitated solids are isolated by centrifugation
  2. stirringwith stirring
  3. customare again recovered by centrifugation
  4. customThe catalyst is dried in a vacuum oven at 50° C.

出典と根拠

ORDレコード
ord-794d40a6200945d3ad81336bfb78cf19
出典データセット
uspto-grants-1998_01
特許番号
US05712216

反応ノート

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