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2,4-Diaminotoluene → HCID 178428252、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4-Diaminotoluene | HCID 7261 | — |
| 反応物 | Nitrosoantipyrine | HCID 13443 | — |
| 反応物 | Sodium Perchlorate | HCID 522606 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178428252 | HCID 178428252 | — |
反応手順
50 mmol of 1,5-dimethyl-4-nitroso-2-phenyl-1,2-dihydro-3H-pyrazol-3-one was dissolved in a solution of 850 ml of acetic acid and 1250 ml of water. This solution was admixed with 50 mmol of 4-methylbenzene-1,3-diamine and stirring was continued for 2 h 30 min. Sodium perchlorate was added to saturation, and the mixture was left to stand for 30 minutes at zero degrees.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07582123B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-337954db342c466cbcef6fe9888bb754 |
| 出典メモ | uspto-grants-2009_09 |