化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Dichloro-2-fluoropyridine → Methyl 4-(N-(benzofuran-6-ylmethyl)-N-(3,5-dichloropyridin-2-yl)sulfamoyl)benzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dichloro-2-fluoropyridine | HCID 2783256 | — |
| 反応物 | Methyl 4-(N-(benzofuran-6-ylmethyl)sulfamoyl)benzoate | HCID 66837871 | — |
| 生成物 | Methyl 4-(N-(benzofuran-6-ylmethyl)-N-(3,5-dichloropyridin-2-yl)sulfamoyl)benzoate | HCID 66837856 | — |
反応手順
The titled compound was prepared according to the procedure described in step-2 of Example 1 from 3,5-dichloro-2-fluoropyridine and methyl 4-(N-(benzofuran-6-ylmethyl)sulfamoyl)benzoate (step-1 of Example 2). LC-MS (method-C) m/z: M+1 obs 490.91; tR=2.75 min.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08829026B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-5cc5d2aa180948738fffc6df6fd0b0e9 |
| 出典メモ | uspto-grants-2014_09 |