化工社化工社 化学情報印刷レポート · 研究参考用
Acetal → 1-(1,4-Dioxa-spiro[4.5]dec-8-yl)-1-(4-methyl-cyclohexyl)-3-(5-methyl-thiazol-2-yl)-urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetal | HCID 7765 | — |
| 反応物 | 4-Methylcyclohexylamine | HCID 80604 | — |
| 反応物 | 2-Amino-5-methylthiazole | HCID 351770 | — |
| 反応物 | 1,4-Dioxaspiro[4.5]decan-8-one | HCID 567415 | — |
| 生成物 | 1-(1,4-Dioxa-spiro[4.5]dec-8-yl)-1-(4-methyl-cyclohexyl)-3-(5-methyl-thiazol-2-yl)-urea | HCID 57883925 | — |
反応手順
1-(1,4-Dioxa-spiro[4.5]dec-8-yl)-1-(4-methyl-cyclohexyl)-3-(5-methyl-thiazol-2-yl)-urea was prepared in an similar manner to example 2 according to general procedures (A) and (B) using 1,4-dioxaspiro[4.5]decan-8-one, 4-methylcyclohexylamine and 2-amino-5-methylthiazole. The acetale was then hydrolysed in the following way:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07582769B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-e43b8a0352204a75bf3fdfcbe0c0c2b5 |
| 出典メモ | uspto-grants-2009_09 |