2-Butoxy-4,6-dichloro-1,3,5-triazine → HCID 66991228、化合物

反応式

[CH2:1]([O:5][C:6]1[N:11]=[C:10](Cl)[N:9]=[C:8](Cl)[N:7]=1)[CH2:2][CH2:3][CH3:4].[CH2:14]([NH:16][C:17]1[CH:18]=[C:19]([OH:23])[CH:20]=[CH:21][CH:22]=1)[CH3:15]>>[CH2:1]([O:5][C:6]1[N:11]=[C:10]([N:16]([CH2:14][CH3:15])[C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([OH:23])[CH:18]=2)[N:9]=[C:8]([N:16]([CH2:14][CH3:15])[C:17]2[CH:22]=[CH:21][CH:20]=[C:19]([OH:23])[CH:18]=2)[N:7]=1)[CH2:2][CH2:3][CH3:4]

参加物

反応物 2

HCID 263022-Butoxy-4,6-dichloro-1,3,5-triazine

HCID 5789913-Ethylaminophenol

生成物 1

HCID 66991228HCID 66991228、化合物収率 47%

実験手順

This compound was obtained (yield 47%) based on the method described in Production Example 1B using 6-butoxy-2,4-dichloro-1,3,5-triazine instead of the 2,4-dichloro-6-ethyl-1,3,5-triazine, and using 3-ethylaminophenol instead of the 3-aminophenol.

後処理

customThis compound was obtained (yield 47%)

出典と根拠

ORDレコード: ord-48b2f4e2baa24c4b91d1d033393e1560
出典データセット: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07589105B2

反応ノート

読み込み中…