化工社化工社 化学情報印刷レポート · 研究参考用
Disodium glutamate → L-Glutamic acid, calcium salt (1:?)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Disodium glutamate | HCID 167560 | — |
| 反応物 | Calcium chloride, dihydrate | HCID 6093260 | — |
| 反応物 | Strontium glutamate | HCID 11390644 | — |
| 反応物 | Sodium L-glutamate hydrate | HCID 23666328 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | L-Glutamic acid, calcium salt (1:?) | HCID 87975 | — |
反応手順
Basically the reaction conditions found for preparation of strontium L-glutamate (Example 8) was employed. A suspension of sodium glutamate (white coloured) is prepared by adding 100 mL of millipore water to 18.714 g (0.1 moles) of solid L-glutamic acid monosodium salt monohydrate (ALDRICH G2834, MW 187.14, CAS 142-47-2) in a 250 mL beaker. To this suspension was added 17.6424 g (0.12 moles) of solid calcium chloride dihydrate (FLUKA, 21097, MW 147.0, CAS 10035-04-8). The reaction procedure described in Example 8 was followed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07589235B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-2d32524033e14a3f9786009e196fb458 |
| 出典メモ | uspto-grants-2009_09 |