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HRID 733742作成日：2026年10月26日

Phosphorodichloridic acid, phenyl ester → Ethyl 4-chloro-1-{[4-(methyloxy)phenyl]methyl}-1H-pyrrolo[3,2-c]pyridine-7-carboxylate

https://huagongshe.com/reaction/733742

反応式

関与物質

役割名称HCID仕込み量
反応物Phosphorodichloridic acid, phenyl esterHCID 13038—
反応物Ethyl 1-{[4-(methyloxy)phenyl]methyl}-4-oxo-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-7-carboxylateHCID 57840819—
生成物Ethyl 4-chloro-1-{[4-(methyloxy)phenyl]methyl}-1H-pyrrolo[3,2-c]pyridine-7-carboxylateHCID 57840887—

反応手順

Prepared in a similar manner to Example 243(e) using ethyl 1-{[4-(methyloxy)phenyl]methyl}-4-oxo-4,5-dihydro-1H-pyrrolo[3,2-c]pyridine-7-carboxylate (14.45 g) and phenyl dichlorophosphate (100 ml) to afford the title compound as a yellow oil (7.2 g).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07589206B2
出典データセットuspto-grants-2009_09
ORD IDord-e85f43810b5b43549820003a70ed2893
出典メモuspto-grants-2009_09