化工社化工社 化学情報印刷レポート · 研究参考用
Benzoyl chloride → 4-Methoxybenzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoyl chloride | HCID 7412 | — |
| 反応物 | Anisole | HCID 7519 | — |
| 生成物 | 4-Methoxybenzophenone | HCID 69146 | 47% |
反応手順
370 mg of benzoylchloride were reacted with 12 ml anisole to give the benzoylated product 4-methoxybenzophenone in 47% yield. The catalyst used is a HS—AlF3 metal fluoride on a Al2O3 support prepared according to the present invention, which is used in an amount of 300 mg. The reaction is carried out in a discontinuous batch process at 60° C. under reflux with stirring.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07592287B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-a14a8e7438594020a2313d82de28bc73 |
| 出典メモ | uspto-grants-2009_09 |