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2-(4-Iodophenyl)ethan-1-ol → HCID 69057844、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(4-Iodophenyl)ethan-1-ol | HCID 3040770 | — |
| 反応物 | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| 生成物 | HCID 69057844 | HCID 69057844 | — |
反応手順
The product was prepared analogously to Example 48.1c from 1.74 g (8.06 mmol) of 5-(4-chlorophenyl)-2-ethynylpyridine and 2.00 g (8.06 mmol) of 2-(4-iodophenyl)ethanol (24 at RT, triethylamine as base and acetonitrile as solvent). Yield: 1.80 g (67% of theoretical); C21H16ClNO (M=333.811); calc.: molpeak (M+H)+:334/336 (Cl); found: molpeak (M+H)+:334/336 (Cl).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07592358B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-e44bce97461e43f191b1396a4b858b0a |
| 出典メモ | uspto-grants-2009_09 |