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2-(2-Fluorophenyl)ethylamine → N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(2-fluorophenyl)-ethyl]amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(2-Fluorophenyl)ethylamine | HCID 643357 | — |
| 反応物 | 4-(Dodecyloxy)-1-naphthaldehyde | HCID 85841201 | — |
| 生成物 | N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(2-fluorophenyl)-ethyl]amine | HCID 67186944 | — |
反応手順
The same procedure as employed in the preparation of Example 394 (step b) but using 4-(dodecyloxy)-1-naphthaldehyde and 2-(2-fluorophenyl)ethylamine gave the title compound as an oil. HPLC (Condition A), Rt: 5.48 min (HPLC purity: 86.4%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07592477B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-ff4a2adcda6c47f987636c761d7ec7eb |
| 出典メモ | uspto-grants-2009_09 |