化工社化工社 化学情報印刷レポート · 研究参考用
2-(Trifluoromethyl)benzylamine → N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(trifluoromethyl)-benzyl]amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Trifluoromethyl)benzylamine | HCID 76447 | — |
| 反応物 | 4-(Dodecyloxy)-1-naphthaldehyde | HCID 85841201 | — |
| 生成物 | N-{[4-(dodecyloxy)-1-naphthyl]methyl}-N-[2-(trifluoromethyl)-benzyl]amine | HCID 67187285 | — |
反応手順
The same procedure as employed in the preparation of Example 394 (step b) but using 4-(dodecyloxy)-1-naphthaldehyde and 2-(trifluoromethyl)benzylamine gave the title compound as an oil. HPLC (Condition A), Rt: 5.54 min (HPLC purity: 98.0%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07592477B2 |
| 出典データセット | uspto-grants-2009_09 |
| ORD ID | ord-c0e8d93f9b7d4f91b93b759d75bdac89 |
| 出典メモ | uspto-grants-2009_09 |