化工社化工社 化学情報印刷レポート · 研究参考用
4-(Chlorodifluoromethoxy)aniline → 6-chloro-N-(4-(chlorodifluoromethoxy)phenyl)-5-iodonicotinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Chlorodifluoromethoxy)aniline | HCID 572793 | — |
| 反応物 | 6-Chloro-5-iodonicotinic acid | HCID 22271477 | — |
| 生成物 | 6-chloro-N-(4-(chlorodifluoromethoxy)phenyl)-5-iodonicotinamide | HCID 86702626 | — |
反応手順
The title compound was prepared in an analogous fashion to that described in Stage 11.2 using 6-chloro-5-iodonicotinic acid and 4-(chlorodifluoromethoxy)aniline to afford an off-white powder. HPLC (Condition 4) tR=6.47 min, UPLC-MS (Condition 3) tR=1.26 min, m/z=456.8 [M−H]−.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08829195B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-f324f55a49224e8a8e5a5fed04932a04 |
| 出典メモ | uspto-grants-2014_09 |