化工社化工社 化学情報印刷レポート · 研究参考用
L-Valinol → N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | L-Valinol | HCID 640993 | — |
| 反応物 | 1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid | HCID 57672890 | — |
| 生成物 | N-[[1-[[(2-Furanylmethoxy)carbonyl]amino]cyclohexyl]carbonyl]L-valinol | HCID 24875907 | — |
反応手順
2.00 g (7.48 mmol) of 1-[[(2-furanylmethoxy)carbonyl]amino]cyclohexanecarboxylic acid was used instead of 2-benzothiophenecarboxylic acid, and 772 mg (7.48 mmol) of L-valinol was used instead of 1-aminocyclohexanecarboxylic acid phenylmethyl ester in the process according to Reference Example 197 to obtain 2.67 g (quantitative) of the title compound and 2.64 g (quantitative) of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08829209B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-2f1ffac19e114f4d97b2ad5ddb4635e3 |
| 出典メモ | uspto-grants-2014_09 |