Hydrochloric Acid → N-(1-methylimidazol-2-yl)benzylideneamine hydrochloride

HRID 741709ノート

反応式

HRID 741709 の反応式
[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[N:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[ClH:15].C(OCC)(=O)C>C(OCC)C>[ClH:15].[CH3:1][N:2]1[CH:6]=[CH:5][N:4]=[C:3]1[N:7]=[CH:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 8857Ethyl AcetateHCID 53843952N-(1-methylimidazol-2-yl)benzylideneamine

生成物 1

HCID 67740815N-(1-methylimidazol-2-yl)benzylideneamine hydrochloride

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

N-(1-methylimidazol-2-yl)benzylideneamine (0.1 g) was dissolved in diethyl ether, and 4N hydrochloric acid--ethyl acetate (0.2 ml) was added. The precipitated pale yellow powder (70.mg, 21.9%) was separated by filtration.

後処理

  1. customThe precipitated pale yellow powder (70.mg, 21.9%) was separated by filtration

出典と根拠

ORDレコード
ord-1e7072fc9e0845de90a53ef38b7a4328
出典データセット
uspto-grants-1996_09
特許番号
US05552427

反応ノート

読み込み中…