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Trichlorooctadecylsilane → 12-[2-[2-(2-Methoxyethoxy)ethoxy]ethoxy]-12-octadecyl-2,5,8,11,13,16,19,22-octaoxa-12-silatricosane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trichlorooctadecylsilane | HCID 8157 | — |
| 反応物 | Triethylene glycol monomethyl ether | HCID 8178 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | 12-[2-[2-(2-Methoxyethoxy)ethoxy]ethoxy]-12-octadecyl-2,5,8,11,13,16,19,22-octaoxa-12-silatricosane | HCID 19427132 | — |
反応手順
The procedure of Example 1 was repeated with 387.5 g (1.0 mole) of octadecyltrichlorosilane and 800 mL of heptane. Under nitrogen 508.4 g (3.10 mole) of 2-(2-(2-methoxyethoxy)ethoxy)ethanol was added at 80° C. over 4 hours. After heating the reaction for an additional 48 hours and removal of all volatile components under vacuum, 780 g of the pale yellow liquid product were obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05552476 |
| 出典データセット | uspto-grants-1996_09 |
| ORD ID | ord-fdac2874a1f24ac4b7ad8403a80d9772 |
| 出典メモ | uspto-grants-1996_09 |