反応式
[C:1]1([OH:7])C=CC=CC=1.[C:8]1(S)C=CC=C[CH:9]=1.Br[C:16]1[N:21]=[C:20]([CH2:22][O:23][Si](C(C)(C)C)(C2C=CC=CC=2)C2C=CC=CC=2)[CH:19]=[CH:18][CH:17]=1.Br[C:42]1C=C(F)C=C(OCC2C=CC(OC)=C(OC)C=2)[CH:43]=1>>[OH:23][C:22]([C:20]1[N:21]=[C:16]([CH2:1][OH:7])[CH:17]=[CH:18][CH:19]=1)([CH2:42][CH3:43])[CH2:8][CH3:9]参加物
5
実験手順
Following the procedure described for Phenol 2, Step 2 and for Phenol 7, Step 3, but substituting 6-bromo(O-tert-butyldiphenylsilyl)pyridin-2-methanol form Step 4 for 1-bromo-3-(3,4-dimethoxybenzyloxy)-5-fluorobenzene, the title compound was obtained.
出典と根拠
- ORDレコード
- ord-5323fae251334457994cf16671f58341
- 出典データセット
- uspto-grants-1996_09
- 特許番号
- US05552437
関連ノート
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