2-(2-(3-Methoxyphenyl)ethyl)phenol → Potassium 2-[2-(3-methoxyphenyl)ethyl]phenolate
反応式
CC(C)([O-])C.[K+:6].[CH3:7][O:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[OH:23])[CH:12]=[CH:13][CH:14]=1>CC(N(C)C)=O>[CH3:7][O:8][C:9]1[CH:10]=[C:11]([CH2:15][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=2[O-:23])[CH:12]=[CH:13][CH:14]=1.[K+:6]参加物
4
実験手順
9.83 g of potassium t-butoxide were added, whilst ice-cooling and stirring, to a solution of 20.0 g of 2-[2-(3-methoxyphenyl)ethyl]phenol (prepared as described in Preparation 20) in 50 ml of dimethylacetamide, and the resulting mixture was stirred at the same temperature for 30 minutes, to give potassium 2-[2-(3-methoxyphenyl)ethyl]phenolate.
後処理
- temperaturecooling
出典と根拠
- ORDレコード
- ord-ace70d24f700402b8a7b86845c571d2b
- 出典データセット
- uspto-grants-1996_09
- 特許番号
- US05556864
反応ノート
読み込み中…