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HRID 7455作成日:2026年10月24日

Benzoate → Benzoate maleate

https://huagongshe.com/ja/reaction/7455

反応式

関与物質

役割名称HCID仕込み量
反応物BenzoateHCID 242—
反応物Maleic AcidHCID 444266—
溶媒Ethyl AcetateHCID 8857—
生成物Benzoate maleateHCID 68560292—

反応手順

In 3 mL of ethyl acetate was dissolved 0.25 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate, and 0.07 g of maleic acid was added thereto, after which the resulting mixture was heated to effect dissolution. The reaction mixture was cooled and the crystals precipitated were collected by filtration to obtain 0.15 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate maleate.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07087594B2
出典データセットuspto-grants-2006_08
ORD IDord-595bfc092f2a49439306456243cac199
出典メモuspto-grants-2006_08