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Benzoate → Benzoate maleate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoate | HCID 242 | — |
| 反応物 | Maleic Acid | HCID 444266 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Benzoate maleate | HCID 68560292 | — |
反応手順
In 3 mL of ethyl acetate was dissolved 0.25 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate, and 0.07 g of maleic acid was added thereto, after which the resulting mixture was heated to effect dissolution. The reaction mixture was cooled and the crystals precipitated were collected by filtration to obtain 0.15 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=benzoate maleate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087594B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-595bfc092f2a49439306456243cac199 |
| 出典メモ | uspto-grants-2006_08 |