Oxalic Acid → Carbonate oxalate
反応式
[C:1](=[O:4])([O-:3])[O-:2].[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7]>C(OCC)(=O)C>[C:5]([OH:10])(=[O:9])[C:6]([OH:8])=[O:7].[C:1](=[O:2])([OH:4])[OH:3]参加物
4
実験手順
In 7 mL of ethyl acetate was dissolved 0.31 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate, and to the solution was added a solution of 0.10 g of oxalic acid in 1 mL of ethyl acetate, after which the resulting mixture was stirred at room temperature. The crystals precipitated were collected by filtration to obtain 0.34 g of 1-{3-[2-(1-benzothiophen-5-yl)ethoxy]propyl}-3-azetidinyl=methyl=carbonate oxalate.
後処理
- customThe crystals precipitated
- filtrationwere collected by filtration
出典と根拠
- ORDレコード
- ord-969acd0d0f2e422ba1015f8da344886c
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07087594B2
反応ノート
読み込み中…