化工社化工社 化学情報印刷レポート · 研究参考用
Phthalic Anhydride → Fluorescein phthalamic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | 5-Aminofluorescein | HCID 76845 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | Fluorescein phthalamic acid | HCID 131714783 | — |
反応手順
A mixture of 350 mg (0.001 mol) of 5-aminofluorescein and 200 mg of phthalic anhydride in 5 milliliters of glacial acetic acid was stirred at ambient temperature for 48 hours. The yellow reddish product was filtered and washed once with acetic acid and twice with diethyl ether. 460 Mg of fluorescein-phthalamic acid was obtained. I.R (KBR) showed bands at 3060; 3000; 1685; 1590; 1540; 1480; 1460; 1430; 1350; 1310; 1270; 1230; 1195; 1150; and 1115 cm-1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04600775 |
| 出典データセット | uspto-grants-1986_07 |
| ORD ID | ord-7cbb0db406bd487cad6863495797162b |
| 出典メモ | uspto-grants-1986_07 |