化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Saccharin | HCID 5143 | — |
| 生成物 | Benzoic acid, 2-(aminosulfonyl)-, methyl ester | HCID 42546 | — |
反応手順
An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04601746 |
| 出典データセット | uspto-grants-1986_07 |
| ORD ID | ord-7682b66929384626b8eedbdba4fb52da |
| 出典メモ | uspto-grants-1986_07 |