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tert-Butyl carbazate → tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | tert-Butyl carbazate | HCID 70091 | — |
| 反応物 | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate | HCID 69201455 | — |
反応手順
A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07393847B2 |
| 出典データセット | uspto-grants-2008_07 |
| ORD ID | ord-b0c24742b0534cffba3d932cbf487f85 |
| 出典メモ | uspto-grants-2008_07 |