N,N-Dimethyl-1,3-propanediamine → HCID 22350930、化合物

HRID 747534ノート

反応式

HRID 747534 の反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8](=[S:12])SCC.[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH2:18]>C(O)C>[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH:18][C:8]([NH:7][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)=[S:12]

参加物

4

反応物 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 12214896Ethyl 2-Pyridyldithiocarbamate

生成物 1

HCID 22350930HCID 22350930、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

A mixture of ethyl 2-pyridyldithiocarbamate (600 mg), 3-(dimethylamino)propylamine (0.38 ml) and ethanol (6 ml) was heated with reflux under nitrogen atmosphere. One and half hour thereafter, the reaction mixture was concentrated under reduced pressure to give the title compound (786 mg) as crude oil.

後処理

  1. temperaturewas heated
  2. temperaturewith reflux under nitrogen atmosphere
  3. concentrationOne and half hour thereafter, the reaction mixture was concentrated under reduced pressure

出典と根拠

ORDレコード
ord-c55300dbfc144f439c6f699b2f6b1245
出典データセット
uspto-grants-2008_07
特許番号
US07396842B2

反応ノート

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