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HRID 747666作成日:2026年10月25日

Hydrochloric Acid → Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride

https://huagongshe.com/reaction/747666

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrochloric AcidHCID 313—
反応物EthanolHCID 702—
反応物Ethyl 4-cyanobenzoateHCID 81589—
溶媒1,4-DioxaneHCID 31275—
生成物Ethyl 4-ethoxycarbonimidoylbenzoate hydrochlorideHCID 68830640—

反応手順

5.16 g (29 mmol) of ethyl 4-cyanobenzoate was stirred in 50 ml of 4N solution of hydrogen chloride in dioxane. 5 ml of ethanol was added to the resultant mixture, and they were stirred at room temperature for 4 days. The solvent was evaporated, and the residue was washed with ethyl acetate and dried to obtain the title compound.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07396844B1
出典データセットuspto-grants-2008_07
ORD IDord-745c474fe6424adb93f48ea986009b47
出典メモuspto-grants-2008_07