化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Ethyl 4-cyanobenzoate | HCID 81589 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride | HCID 68830640 | — |
反応手順
5.16 g (29 mmol) of ethyl 4-cyanobenzoate was stirred in 50 ml of 4N solution of hydrogen chloride in dioxane. 5 ml of ethanol was added to the resultant mixture, and they were stirred at room temperature for 4 days. The solvent was evaporated, and the residue was washed with ethyl acetate and dried to obtain the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07396844B1 |
| 出典データセット | uspto-grants-2008_07 |
| ORD ID | ord-745c474fe6424adb93f48ea986009b47 |
| 出典メモ | uspto-grants-2008_07 |