HCID 17788760、化合物 → 3-(3-Cyanophenoxy)propanoic acid
反応式
[C:1]([C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][CH:15]=1)[O:6][CH2:7][CH2:8][C:9]([O:11]C)=[O:10])#[N:2]>Cl>[C:1]([C:3]1[CH:4]=[C:5]([CH:13]=[CH:14][CH:15]=1)[O:6][CH2:7][CH2:8][C:9]([OH:11])=[O:10])#[N:2]参加物
3
実験手順
500 mg (2.4 mmol) of methyl 3-(3-cyanophenoxy)propionate was heated in 40 ml of 6 N hydrochloric acid at 70° C. for 30 minutes. After the extraction with ethyl acetate, the extract was washed with saturated aqueous NaCl solution and then dried on anhydrous magnesium sulfate. The solvent was evaporated to obtain the title compound.
後処理
- extractionAfter the extraction with ethyl acetate
- washthe extract was washed with saturated aqueous NaCl solution
- dry with materialdried on anhydrous magnesium sulfate
- customThe solvent was evaporated
出典と根拠
- ORDレコード
- ord-a0f90bcfe61f4b89968b8c87665793a1
- 出典データセット
- uspto-grants-2008_07
- 特許番号
- US07396844B1
反応ノート
読み込み中…