化工社化工社 化学情報印刷レポート · 研究参考用
Methacrylic Acid → Methacrylic acid hydroxypropyl methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methacrylic Acid | HCID 4093 | — |
| 反応物 | Tetrahydrofuran | HCID 8028 | — |
| 反応物 | 3-Hydroxypropyl methacrylate | HCID 17694 | — |
| 触媒 | Azobisisobutyronitrile | HCID 6547 | — |
| 溶媒 | Diethylethylether | HCID 12430074 | — |
| 生成物 | Methacrylic acid hydroxypropyl methacrylate | HCID 86602182 | 582.3% |
反応手順
To 20 g of THF were added 9 g of methacrylic acid, 1 g of hydroxypropyl methacrylate, and 0.1 g of AIBN. The resulting mixture was reacted at 67° C. for 3 hours. After reaction, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.3 g of a photoresist polymer of Formula (IVd).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07399570B2 |
| 出典データセット | uspto-grants-2008_07 |
| ORD ID | ord-a4dcbc86eb9c458dae976a088d9d0c1d |
| 出典メモ | uspto-grants-2008_07 |