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2-(Phenylmethyl)propanedinitrile → 2-benzyl-2-((E)-3-chloro-2-propenyl)malononitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-(Phenylmethyl)propanedinitrile | HCID 15846 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | 1,3-Dichloropropene | HCID 24883 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 2-benzyl-2-((E)-3-chloro-2-propenyl)malononitrile | HCID 22235007 | 36.4% |
反応手順
Using 0.49 g of benzylmalononitrile, 15 ml of N,N-dimethylformamide, 0.14 g of sodium hydride (60% in oil), and 0.33 g of 1,3-dichloropropene, and according to the process described in the Production Example 1, there was obtained 0.25 g of 2-benzyl-2-((E)-3-chloro-2-propenyl)malononitrile (the present compound (60)) as high-polar compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07402691B2 |
| 出典データセット | uspto-grants-2008_07 |
| ORD ID | ord-d4b7bbe000b04ae5a60a261f8538481a |
| 出典メモ | uspto-grants-2008_07 |