化工社化工社 化学情報印刷レポート · 研究参考用
4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
反応手順
A large excess of thionyl chloride was added to 10 g of the p-octyloxybenzoic acid prepared in (1), and the mixture was refluxed for 5 hours. Excessive thionyl chloride was distilled off to give a crude end compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05723069 |
| 出典データセット | uspto-grants-1998_03 |
| ORD ID | ord-89aff4b1c18042e4bbb1f88ebba96f86 |
| 出典メモ | uspto-grants-1998_03 |