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Benzaldehyde → HCID 178418819、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | 2-Aminothiazole | HCID 2155 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | Tert-Butyl isocyanide | HCID 23577 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | HCID 178418819 | HCID 178418819 | — |
反応手順
Example 4 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-thiazole (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087607B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-3530e699346948b5a62efd1270abe4aa |
| 出典メモ | uspto-grants-2006_08 |