1-Butanaminium, N,N,N-tributyl-, fluoride, hydrate → (7-Hydroxy-indol-1-yl)-acetic acid ethyl ester
反応式
[CH2:1]([O:3][C:4](=[O:23])[CH2:5][N:6]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][C:13]=2[O:15][Si](C(C)(C)C)(C)C)[CH:8]=[CH:7]1)[CH3:2].O.[F-].C([N+](CCCC)(CCCC)CCCC)CCC>>[CH2:1]([O:3][C:4](=[O:23])[CH2:5][N:6]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][C:13]=2[OH:15])[CH:8]=[CH:7]1)[CH3:2]参加物
3
実験手順
In analogy to the procedure described in example 6 c], [7-(tert-butyl-dimethyl-silanyloxy)-indol-1-yl]-acetic acid ethyl ester was treated with tetrabutylammonium fluoride hydrate to give the title compound as colorless solid.
出典と根拠
- ORDレコード
- ord-3367a52c6b8f43d4985446b56cff5a77
- 出典データセット
- uspto-grants-2008_07
- 特許番号
- US07405236B2
反応ノート
読み込み中…