化工社化工社 化学情報印刷レポート · 研究参考用
Acetaldehyde → HCID 178418843、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetaldehyde | HCID 177 | — |
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | Cyclohexyl isocyanide | HCID 79129 | — |
| 反応物 | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | HCID 178418843 | HCID 178418843 | — |
反応手順
Example 7 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-3-benzyloxypyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087607B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-efb2df06a3ae44799f8795ccf59d72ac |
| 出典メモ | uspto-grants-2006_08 |