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Acetyl chloride → HCID 178418859、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetyl chloride | HCID 6367 | — |
| 反応物 | 2-Aminopyridine | HCID 10439 | — |
| 反応物 | Cyclohexanecarboxaldehyde | HCID 16275 | — |
| 反応物 | Cyclohexyl isocyanide | HCID 79129 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | HCID 178418859 | HCID 178418859 | — |
反応手順
Example 23 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) cyclohexane carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087607B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-d6b7304d14924773a356ec02ce0f21c6 |
| 出典メモ | uspto-grants-2006_08 |